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Solvent Microextractio
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Specificaties
- Objectstaat
- Book Title
- Solvent Microextraction: Theory and Practice
- Publication Date
- 2009-10-01
- Pages
- 344
- ISBN
- 9780470278598
- Publication Year
- 2009
- Type
- Textbook
- Format
- Hardcover
- Language
- English
- Publication Name
- Solvent Microextraction : Theory and Practice
- Item Height
- 0.8in
- Item Length
- 9.6in
- Publisher
- Wiley & Sons, Incorporated, John
- Item Width
- 6.4in
- Item Weight
- 21.5 Oz
- Number of Pages
- 344 Pages
Over dit product
Product Information
ADD SOLVENT MICROEXTRACTION TO YOUR ANALYTICAL TOOLKIT WITH THIS HANDS-ON GUIDE This timely resource turns solvent microextraction (SME) into a practical analysis tool that analytical chemists will find to be a powerful adjunct to established sample preparation methods. Whether youre involved in sample preparation and analysis of solid, liquid, or atmospheric environmental, clinical, or industrial samples, Solvent Microextraction: Theory and Practice includes the information you need to integrate this cutting-edge sample preparation technique into your everyday practice, including: Insightful comparisons with other popular sampling methods A theoretical discussion of SME, supported by examples of how theory impacts real samples An extensive bibliography of nearly 600 application references, updated to 2009 A detailed compilation of experimental parameters and summaries of published procedures to aid in method development More than a dozen experimental procedures for the most commonly used SME modes, with an emphasis on how to effectively apply the technique SME modes classification and glossary to facilitate further study and research A skill-sharpening CD-ROM that contains summaries of nearly 600 publications using SME Written by the leading experts on SME technology, Solvent Microextraction is a time- and money-saving sourcebook that serves as both a convenient desk reference for the laboratory and an indispensable teaching tool. Most importantly, it goes beyond a compilation of reference material, providing you with a much-needed guide to proper experimental procedures, and a blueprint for understanding how and why the SME technique works.
Product Identifiers
Publisher
Wiley & Sons, Incorporated, John
ISBN-10
0470278595
ISBN-13
9780470278598
eBay Product ID (ePID)
73208258
Product Key Features
Publication Name
Solvent Microextraction : Theory and Practice
Format
Hardcover
Language
English
Publication Year
2009
Type
Textbook
Number of Pages
344 Pages
Dimensions
Item Length
9.6in
Item Height
0.8in
Item Width
6.4in
Item Weight
21.5 Oz
Additional Product Features
Number of Volumes
1 Vol.
Lc Classification Number
Qd63.E88k65 2009
Reviews
"The present book constitutes a unique source for the analyst that may find a useful compilation of reference material, a guide to proper experimental procedures, and a better understanding of how and why the technique works." (Chemistry Journals, 11 April 2011) "Written by three pioneers and worldwide recognised specialists in the field, this timely monograph is not only an exhaustive and updated compilation of bibliography related to solvent microextration techniques and their applications in different work areas, but a practical and useful guide for all those interested in their direct application to practical case studies." (Chromatographia, 1 December 2010) "Describe[s] procedures and applications of the research technique, which in the past dozen or so years has grown beyond academic laboratories to find work in industrial, forensic, clinical, and environmental analysis." ( Book News , December 2009)
Table of Content
PREFACE. 1 SOLVENT MICROEXTRACTION: COMPARISON WITH OTHER POPULAR SAMPLE PREPARATION METHODS. 1.1 Introduction. 1.2 Comparison of Sample Preparation Methods. 1.3 Summary. References. 2 BASIC MODES OF OPERATION FOR SOLVENT MICROEXTRACTION. 2.1 Basic Principles of SME. 2.2 Extraction Modes. 2.3 Solvents. 3 THEORY OF SOLVENT MICROEXTRACTION. 3.1 Introduction. 3.2 Thermodynamics. 3.3 Kinetics. 3.4 Calibration Methods. 3.5 Summary. References. 4 PRACTICAL CONSIDERATIONS FOR USING SOLVENT MICROEXTRACTION. 4.1 Introduction. 4.2 General Recommendations. 4.3 General Questions to Consider Before Performing an Analysis. 4.4 Choosing the SME Mode. 4.5 Extraction Solvent. 4.6 Sample Volumes. 4.7 Syringe and Microdrop. 4.8 Chromatography and Detector Requirements. 4.9 Additional Extraction Parameters. 4.10 Calculation Examples for SDME. 4.11 Calculation Examples for DLLME and HFME. 4.12 Calculation Examples for the Effect of Ionic Strength on SDME. 4.13 Calculation Examples for HS-SDME. 4.14 Calculation Examples for the Effect of Ionic Strength on HS-SDME. 4.15 Calculation Examples for Static Headspace Extraction. 4.16 Calculation Examples for Solvent Solubility. References. 5 METHOD DEVELOPMENT IN SOLVENT MICROEXTRACTION. 5.1 Introduction. 5.2 Extraction Mode Selection. 5.3 Static vs. Dynamic Extraction. 5.4 Selection of Manual vs. Automated Extraction. 5.5 Selection of Direct vs. Derivatization SME. 5.6 Extraction Solvent Selection. 5.7 Selection of Final Determination Method. 5.8 Selection of Extraction Optimization Method. 5.9 Optimization of Extraction Conditions. References. 6 APPLICATIONS. 6.1 Introduction. 6.2 Gaseous Samples. 6.3 Liquid Samples. 6.4 Solid Samples. 6.5 Environmental Applications of SME. 6.6 Clinical and Forensic Applications of SME. 6.7 Application of SME in Food and Beverage Analysis. 6.8 Application of SME in the Analysis of Plant Material. 6.9 Application of SME in the Analysis of Consumer Products and Pharmaceuticals. 6.10 Outlook for Future Analytical Applications of SME. 6.11 Physicochemical Applications of SME. References. 7 SME EXPERIMENTS. 7.1 Introduction. 7.2 Recommended Experimental Conditions. 7.3 Determination of Gasoline Diluents in Motor Oil by HS-SDME. 7.4 Determination of BTEX in Water by HS-SDME. 7.5 Analysis of Halogenated Disinfection By-Products by SDME and HS-SDME. 7.6 Analysis of Volatile Organic Compounds by SDME and HS-SDME. 7.7 Analysis of Residual Solvents in Drug Products by HS-SDME. 7.8 Arson Accelerant Analyses by HS-SDME. 7.9 Analysis of PAHs by SDME. 7.10 Determination of Acetone in Aqueous Solutions by Derivatization HS-SDME. 7.11 Determination of Pesticides in Soil by HF(2)ME. 7.12 Determination of PAHs and HOCs by DLLME. 7.13 Dynamic Headspace and Direct Immersion Extractions (DY-SME). References. ACRONYMS AND ABBREVIATIONS. APPENDIX SME MODES: CLASSIFICATION AND GLOSSARY. INDEX.
Copyright Date
2009
Topic
Chemistry / Analytic
Lccn
2009-009768
Dewey Decimal
660/.284248
Intended Audience
Scholarly & Professional
Dewey Edition
22
Illustrated
Yes
Genre
Science
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